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Title of Article

APPLICATION OF ATMOSPHERIC MOISTURE IN CONDENSATION FOCUSING OF BENZENE AND ITS HOMOLOGUES FOR THEIR DETERMINATION IN THE AIR BY GAS CHROMATOGRAPHY-MASS SPECTROMETRY


Issue
3
Date
2012

Article type
scientific article
UDC
543.27.05
Pages
92-98
Keywords
air analysis, condensate preconcentration, aromatic hydrocarbons, chromatography-mass spectrometry


Authors
Krylov Valentin Alekseevich
Nizhegorodskiy gosuniversitet im. N.I. Lobachevskogo, Institut khimii vysokochistykh veschestv im. G.G. Devyatykh RAN, Nizhniy Novgorod

Mosyagin Pavel Valerevich
Nizhegorodskiy gosuniversitet im. N.I. Lobachevskogo


Abstract
A method for preconcentration of aromatic hydrocarbons from the air has been developed. The method is based on the use of atmospheric moisture as a natural collector of impurities from the air. The impurities were extracted from the condensed moisture by means of liquid microextraction. The integral factor of the aromatic hydrocarbon condensate preconcentration was (2–6)•104. The extract was analyzed by gas chromatography-mass spectrometry. The detection limits achieved were in the range of 1•10-5–3•10-5 µg/m3.

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