SEARCH FOR OPTIMAL CONDITIONS OF TRIMETHYLGALLIUM SYNTHESIS BY DIRECT REACTION OF A MIXTURE OF GALLIUM AND MAGNESIUM METALS WITH METHYL IODIDE IN ETHER SOLUTION |
| 5 | |
| 2012 |
| 54.057:547.1’1681’211 | |||
| 103-109 |
| The results of the study to obtain trimethylgallium by direct reaction of a Ga-Mg mixture with methyl iodide in the amyl ether solution are presented. It has been shown that the production of trimethylgallium is substantially affected by by-product processes such as the Wurtz reaction of methyl iodide with organometallic compounds and metallic gallium agglomeration. The optimal molar ratio of initial reagents has been found to be Ga:Mg:CH
3I = = 1:3:6. |
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